1 Crystal Geometry. I. - 1. 1 Introduction. - 1. 2 The Crystalline State. - 1. 3 Stereographic Projection. - 1. 4 External Symmetry of Crystals. - Problems. - 2 Crystal Geometry. II. - 2. 1 Introduction. - 2. 2 Lattices. - 2. 3 Families of Planes and Interplanar Spacings. - 2. 4 Reciprocal Lattice. - 2. 5 Rotational Symmetries of Lattices. - 2. 6 Space Groups. - Problems. - 3 Preliminary Examination of Crystals by Optical and X-Ray Methods. - 3. 1 Introduction. - 3. 2 Polarized Light. - 3. 3 Optical Classification of Crystals. - 3. 4 Direction of Scattering of X-Rays by Crystals. - 3. 5 X-Ray Techniques. - Problems. - 4 Intensity of Scattering of X-Rays by Crystals. - 4. 1 Introduction. - 4. 2 Path Difference. - 4. 3 Combination of Two Waves. - 4. 4 Argand Diagram. - 4. 5 Combination of N Waves. - 4. 6 Combined Scattering of X-Rays from the Contents of the Unit Cell. - 4. 7 Structure Factor. - 4. 8 Intensity Expressions. - 4. 9 Phase Problem in Structure Analysis. - 4. 10 Applications of the Structure Factor Equation. - 4. 11 Preliminary Structure Analysis. - Problems. - 5 Methods in X-Ray Structure Analysis. I. - 5. 1 Introduction. - 5. 2 Analysis of the Unit-Cell Contents. - 5. 3 Two Early Structure Analyses Revisited. - Problems. - 6 Methods in X-Ray Structure Analysis. II. - 6. 1 Introduction. - 6. 2 Fourier Series. - 6. 3 Representation of Crystal Structures by Fourier Series. - 6. 4 Methods of Solving the Phase Problem. - Problems. - 7 Some Further Topics. - 7. 1 Introduction. - 7. 2 Direct Methods of Phase Determination. - 7. 3 Least-Squares Refinement. - 7. 4 Molecular Geometry. - 7. 5 Accuracy. - 7. 6 Correctness of a Structure Analysis. - 7. 7 Anomalous Scattering. - 7. 8 Limitations of X-Ray Structure Analysis. - Problems. - 8 Examplesof Crystal Structure Analysis. - 8. 1 Introduction. - 8. 2 Crystal Structure of 2-Bromobenzo[b]indeno[32-e]pyran (BBIP). - 8. 3 Crystal Structure of Potassium 2-Hydroxy-34-dioxocyclobut-1-ene-1-olate Monohydrate (KHSQ). - 8. 4 Concluding Remarks. - Problems. - A. 1 Stereoviews and Crystal Models. - A. 1. 1 Stereoviews. - A. 1. 2 Model of a Tetragonal Crystal. - A. 2 Crystallographic Point-Group Study and Recognition Scheme. - A. 3 Schoenflies' Symmetry Notation. - A. 3. 1 Alternating Axis of Symmetry. - A. 3. 2 Notation. - A. 4 Generation and Properties of X-Rays. - A. 4. 1 X-Rays and White Radiation. - A. 4. 2 Characteristic X-Rays. - A. 4. 3 Absorption of X-Rays. - A. 4. 4 Filtered Radiation. - A. 5 Crystal Perfection and Intensity Measurement. - A. 5. 1 Crystal Perfection. - A. 5. 2 Intensity of Reflected Beam. - A. 5. 3 Intensity Measurements. - A. 5. 4 Intensity Corrections. - A. 6 Transformations. - A. 7 Comments on Some Orthorhombic and Monoclinic Space Groups. - A. 7. 1 Orthorhombic Space Groups. - A. 7. 2 Monoclinic Space Groups. - Solutions. Language: English